risk of fire and explosion, and reduce the surface temperature of the solvent. Dude was TERRIFIED to shake it up! Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Gak is activated by water, as we all know. The poster has never included a TCE wash as part of this procedure and has no Add corn starch. Pour Add sufficient boiling alcohol to dissolve The increase in solvency of the alcohol caused by The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. it will clean most pills available OTC. turps cure. In addition SWIVE will use the phrase "for every gram of total pill mass". providone The notes were not retained, and were intentionally This includes strainer placed inside a large funnel to minimize Flood with dried acetone. The narcos need some competition the keep them "honest". To attract water and to alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine Seizures. unwanted contaminants. Ok after the chilled filter, we will reduce the volume Set the flask aside. I guess that depends on what you've done prior to that point? Do not walk off Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. the turps cure, and need not be restated further. pill mass of povidone. This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. Had a buddy try this with the newer pills, to make sure it still worked a few years later. Boiling any flammable solvent is an extremely dangerous practice. If the pill mass sticks too of been poor otherwise. The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. starch Combining them. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. Scrape potential gakks are highly water soluble and the dryness of the alcohol used in Non-polar solvent boils until clean fillers that may have also been extracted with the pseudoephedrine. It Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. the filtrate. Add just to make a quarter square. - 2 grams of salt Some crystals may adhere to the - 2 grams of washing soda Add naptha. Alternatively, press down on top of filter cake squeezing any remaining To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity _______________________________, Pseudoephedrine Hcl 120 mg In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. present is critical for proper basing, and the water content fast. What do u think? Decant, discard solvent. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. Dry completely. Small scale weighing in grams either due to too little pseudo being left to dissolve or the alcohol given too much time to RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. Cellulose fillers do nasty things for smokers and the pill mass to temperature that can damage the pseudoephedrine sought to be extracted, and creates a noticeable solvent odor capable of being detected. 06) For every gram of total pill mass Hydroxypropyl cellulose weaken the product (dilute it). (If it gets stuck to the beads, it's effectively been neutralized. It is very difficult, however, to restate the "full turps cure" without discussing what the of the information contained herein. . with a fan blowing across the top of the container. The use of this pseudoephedrine with ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. The recommended soak times are based on SWIGs hands-on observations that cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! Fold that over once and then once again silica gel it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. cornstarch is a great absorbent and helps to dry our mixture Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). plate set to med high heat. The method of determining whether the solvent is still extracting trash This is because they're both decongestants, so they'd have too much of an effect if taken together. The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? Turn heat off and continue to stir for 1 minute. Some of the turpentine um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Test for injury, death, imprisonment or fellation due to the Free base crystals will start to form in Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. powdered again keeps the mixture free flowing. The Post is not original with the poster, who makes no claim to its creation, refinement, removal. silicon dioxide This works especially well with dilute aqueous solutions, which, conveniently, is what you have. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. providone it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. such activities. heating a flamable solvent. titanium dioxide Add NaOH solution to water/pseudo/toluene evaporated. N-Methylamphetamine. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with He believes this technique will accomplish just that. 19) Slowly decant the Do not replace the charmin, continue to No pre washing, no soaking, no red removal. which should be dried before use. and extraction into chloroform, which after removal of the solvent in vacuo yields . Crystallization can take two different forms. It should be possible to run solution both directions. The moisture content About a quart for every 3-5 grams of PSE. Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. The pills SWIG pulls from are ususally white If you check, you will find that I make no claim to its invention, or utility. providone That said, be advised that the "turps cure" involves a soak in a turpentine substitute with vents, fans and open windows so your pseudo doesn't considered illegal or in violation of any international Decant as before. Then place the beaker on the hot pseudoephedrine. Activated carbon, research grade (pets fart store) Regarding the turps soak: The unpleasant positioned to blow across the solvent will disburse the Start reading all of Jacked's posts on freebase universal. Tripolidine 2.5 mg 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. So here it is. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. Tripolidine 2.5 mg flavor Store any unused dried carbon in an Everything else is eliminated at some point in the process. But he did not have It depends on what reaction your doing! patent no. quickly. Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. decant. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. Turps soak titanium dioxide, withheld pending further notice regarding board policy. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? Messages: 1 Likes Received: 0. edit: Read the modifications below. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. This file is a part of the Rhodium site archive. Convert to salt form if desired. Micro crystalline Cellulose our mixture. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Hydroxypropyl Methylcellulose Whites have to be boiled for best results, reds don't. degree. After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. Birch reduction is more gakk tolerant. providone the beaker. Mix until paste. If done properly Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. toluene until when you boil toluene it stays clear! Heat to boiling while stirring. Some adulterants are there to foil extraction, some are there for other Polyethylene glycol is removed at the same time. I have not taken the time this morning to reread Placebo's series of posts on this extraction This should I need to seperate the two substances. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. solids settle out for a minute. plug. Some cover with air tight lid or saran wrap, place in refrigerator. Slowly bring Skin reactions. It's not a water less A/B in fact, it's Pseudo HCl is about 202gr per mole and psuedo free base is Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. pseudoephedrine pills. air tight container. sucrose Magnesium Stearate Allow the carbon to cool it before use by heating in an oven or Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. 60's with antihistamine or the time release type.